Investigation of a U(IV)/U(III) Thermodynamic Reference Electrode for High-Temperature Molten Fluoride Salts
This peer-reviewed publication presents the development of a high-temperature reference electrode for molten fluoride salts.
The work demonstrates production and characterization of exceptionally pure FLiBe, including free oxide concentrations below 2 ppm and low trace-metal contamination. It describes analytical methods for impurity characterization and the importance of purified FLiBe for accurate and reproducible electrochemical measurements.
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Gunnell, E., Blackwood, B. L., Wilson, C., Harb, J. N., & Memmott, M. J. Investigation of a U(IV)/U(III) Thermodynamic Reference Electrode for High-Temperature Molten Fluoride Salts. Journal of The Electrochemical Society, 2025.